Soot: How Much is too Much?

Blackstone offers percent soot testing as an optional test above and beyond what we do in the standard analysis. It’s something many of our diesel customers have shown interest in. It can be challenging for people to understand how much soot is a problem and how much is normal, so in this article we’ll shed some light on our testing process and what it can tell you about the health of your engine.

Here’s a brief run-down of how it works. We use an FTIR (Fourier Transform Infrared) spectrometer to measure the  percentage of soot present in an oil sample. Essentially, soot raises the absorption rate of the infrared light spectrum and when an infrared beam is shot through the sample, the rate of absorption is measured and quantified. The lab operator ensures the machine is running properly by performing a series of check standards, including calibrating against a known 2.0% soot sample to ensure accuracy.

Okay, nap-time is over. So what is soot and what impact can it have on an engine? Soot is a natural by-product of internal combustion. Soot is the reason diesel engine oil turns black, sometimes only after a few miles. When it becomes excessive it can thicken up the viscosity, leave deposits on wearing components, and ultimately clog a filter (or perhaps worse, an oil passage). Excess soot can have an abrasive component and has the ability to stick to wearing surfaces, potentially increasing oil consumption.

A used sample from a Volkswagen 2.0L TDI. Soot reads at 0.4%.

We like to see soot at 1.0% or less; anything higher than 2.0% to be cautionary. So what does that mean to you? In layman’s terms, excess soot can indicate a combustion problem. Pinpointing that problem (or problems) can be a bit more difficult, but there are a couple fairly simple things to check if you think you’re seeing excess (or just more than normal) soot in the oil. Make sure that the fuel system is maintained and properly calibrated so that the injectors are operating at peak efficiency and with a proper air/fuel ratio. Also check for intake leaks and make sure that the air filter is clean and serviceable. Make sure injection timing is set correctly as well. Change the oil and filter regularly to prevent soot build-up.

It’s always possible that excess soot is due to a mechanical problem too, and that’s obviously a bit more involved than just changing the oil or swapping out a dirty air filter. Excessive ring clearance is a common cause of excess soot. Keep an eye on oil consumption as increases in that area can also show a developing ring problem.

Several of our customers have installed by-pass filtration systems in an effort to keep soot lower and the oil cleaner in general, and that can be effective. Employing an oil analysis regimen can also be helpful in assessing wear metals and other contamination like soot…but as a Blackstone customer, you already knew that!

By |2024-09-19T10:22:07-04:002023|Articles, Gas/Diesel Engine, Lab Tests|Comments Off on Soot: How Much is too Much?

What are Insolubles?

The insolubles test measures the total insoluble materials in an oil sample — that is, all solid or liquid materials that are not soluble (won’t mix) in with the oil. We test insolubles using the centrifuge method. A measured volume of oil is mixed with a heated solvent, agitated, and spun at high speed. Insoluble materials collect at the bottom of a tapered glass test tube and can then be quantified. The insolubles level indicates how fast the oil is oxidizing and how effectively the oil filtration system is functioning.

Virgin oils shouldn’t have more than a trace of insolubles in them. The insolubles in virgin oils are from the normal oxidation process of the oil, which leaves free carbon in suspension when oxygen forms with hydrogen (oil is a hydrocarbon). Or they can be from additives that have fallen out of suspension.

Industrial oil normally contains a very low level of insolubles due to the few and relatively mild heat cycles the oil experiences (heat cycles accelerate the oil’s normal tendency to oxidize). Further, oil filtration on industrial machines may filter particles as small as 2 to 10 microns, keeping the oil pristine for a very long time, often years.

Automotive and aircraft oils however, suffer the most difficult environmental problems of all types of oils we analyze. They regularly receive blow-by products from the combustion process, and they suffer extreme heat cycles. Any contaminant will accelerate the oxidation process, causing insoluble materials to increase. Because excessive solid material in the oil limits the oil’s ability to lubricate effectively, an engine oil with a high level of insoluble material needs to be changed.

Excessive insolubles can form if the oil or engine is running hot, is receiving more than a normal amount of contamination or blow-by, is suffering more (or more severe) heat cycles than is normal, is being run longer than a typical use cycle, or, on the other side of the coin, if oil filtration is marginal or relatively ineffective.

If we found no contamination in your oil and your oil change intervals are normal, we often mention a problem at oil filtration as a possible cause of higher insolubles. Your oil filter may be inferior, or it is possible the oil filter bypass valve has relieved if the filter is becoming restricted. The filter system bypass may also open upon unusually cold starts when the oil is too thick to pass through the filter media. Once the bypass relieves, the filter is effectively out of the system.

The insolubles test is a fair measure of several possible problems in your engine. One high reading needn’t be a cause of concern. Several high readings in a row merit investigation of what the problem may be.

By |2024-09-19T10:45:32-04:002023|Articles, Lab Tests|Comments Off on What are Insolubles?
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