What is a Flashpoint?

We use the flashpoint test to determine how much fuel dilution is present in your oil. Technically speaking, the flashpoint is the lowest temperature at which a liquid will generate sufficient vapor to flash (ignite) when exposed to a source of ignition or fire. In other words, at what temperature do the vapors coming off your oil catch fire? For most gasoline oil samples, it’s around 380°F. For most diesel samples, it’s about 410°F.

Each brand/type of oil has an expected “should be” value for the flashpoint, and when the lab test results read lower than that value, it shows a contaminant in the oil. Most often that contaminant is fuel, though other things can affect the flashpoint too, such as solvents (like engine cleaner additives) or water. We calculate the amount of fuel present based on where the flashpoint is relative to the “should be” value and the volatility of the type of fuel you’re using in the engine. Alternative fuels like B20 can have a different impact on the flashpoint than standard fuels, so be sure to let us know if you’re using anything other than standard gas/diesel as fuel in your engine.

Based on the margin of error for the methodology we use for measuring the flashpoint, the lowest fuel dilution value you’ll see on one of our reports is <0.5%. That’s our way of essentially saying that no measurable fuel dilution was detected in the oil. If the flashpoint of your sample reads the same as the “should be” value, we’ll report a “TR” (or trace) of fuel dilution. In other words, it’s likely there was a very small amount of fuel dilution present, but not enough to quantify. After that, you’ll see fuel dilution reported as a percentage of the sample. The most fuel our test can accurately read is 10%. If you have more than that, we’ll report >10% (and you should head to a mechanic).

How much fuel is too much? It depends. We have different allowances for different types of engines based on their typical operational conditions, and we share those values in the “should be” column. If you’re constantly exceeding those values, you might consider the type of operation the engine sees just before sampling. Are you idling the engine to warm it up? Have you just been running errands around town? Is the dealer changing your oil (and starting your engine briefly to pull the vehicle onto a lift)? That type of operation can introduce a little fuel dilution into the oil and as such isn’t necessarily a concern. If the amount of fuel in the oil is consistently above 2.0-3.0%, or if it’s increasing from sample to sample, that might indicate a more serious problem.

A little fuel dilution – the type you’d get in your oil from operational factors — will cook out of the oil once the oil reaches operational temperature. If there’s a fuel dilution problem, though, you’ll see telltale signs: a rising oil level, high fuel dilution readings in testing, a strong fuel smell to the oil, and possibly low viscosity readings and increasing wear as well. The concern with excessive fuel dilution is that it dilutes and thins the oil, which might limit the oil’s ability to effectively protect and cool your engine.

By |2024-09-19T10:43:23-04:00July 13, 2023|Articles, Lab Tests|Comments Off on What is a Flashpoint?

What are Insolubles?

The insolubles test measures the total insoluble materials in an oil sample — that is, all solid or liquid materials that are not soluble (won’t mix) in with the oil. We test insolubles using the centrifuge method. A measured volume of oil is mixed with a heated solvent, agitated, and spun at high speed. Insoluble materials collect at the bottom of a tapered glass test tube and can then be quantified. The insolubles level indicates how fast the oil is oxidizing and how effectively the oil filtration system is functioning.

Virgin oils shouldn’t have more than a trace of insolubles in them. The insolubles in virgin oils are from the normal oxidation process of the oil, which leaves free carbon in suspension when oxygen forms with hydrogen (oil is a hydrocarbon). Or they can be from additives that have fallen out of suspension.

Industrial oil normally contains a very low level of insolubles due to the few and relatively mild heat cycles the oil experiences (heat cycles accelerate the oil’s normal tendency to oxidize). Further, oil filtration on industrial machines may filter particles as small as 2 to 10 microns, keeping the oil pristine for a very long time, often years.

Automotive and aircraft oils however, suffer the most difficult environmental problems of all types of oils we analyze. They regularly receive blow-by products from the combustion process, and they suffer extreme heat cycles. Any contaminant will accelerate the oxidation process, causing insoluble materials to increase. Because excessive solid material in the oil limits the oil’s ability to lubricate effectively, an engine oil with a high level of insoluble material needs to be changed.

Excessive insolubles can form if the oil or engine is running hot, is receiving more than a normal amount of contamination or blow-by, is suffering more (or more severe) heat cycles than is normal, is being run longer than a typical use cycle, or, on the other side of the coin, if oil filtration is marginal or relatively ineffective.

If we found no contamination in your oil and your oil change intervals are normal, we often mention a problem at oil filtration as a possible cause of higher insolubles. Your oil filter may be inferior, or it is possible the oil filter bypass valve has relieved if the filter is becoming restricted. The filter system bypass may also open upon unusually cold starts when the oil is too thick to pass through the filter media. Once the bypass relieves, the filter is effectively out of the system.

The insolubles test is a fair measure of several possible problems in your engine. One high reading needn’t be a cause of concern. Several high readings in a row merit investigation of what the problem may be.

By |2024-09-19T10:45:32-04:00July 13, 2023|Articles, Lab Tests|Comments Off on What are Insolubles?
Go to Top